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Using bis(pinacolato)diboron (B 2 Pin 2 ) under catalytic [Ir(COD)OMe] 2 and 4,4′-di-tert-butyl-2,2′-dipyridyl (dtbpy) as the ligand in absolute heptane at 80 °C for ≥17 h, C12-boronate ester 1 was obtained as the single isomer (Fig
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